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022722 Vancomycin Aglycon Trifluoroacetic Acid Salt Hydrate CAS:

Specifications
References
Grade
Highly Purified
Molecular Formula
C55H52Cl2F3N8O18 xH2O
Molecular Weight
1240.95
EU Commodity Code
38220090
Shipping Temp
Blue Ice
Storage Temp
-20°C
22H-8,11:18,21-Dietheno-23,36-(iminomethano)-13,16:31,35-dimetheno-1H,16H-[1,6,9]oxadiazacyclohexadecino[4,5-m][10,2,16]benzoxadiazacyclotetracosinevancomycin Aglycone Derivative Trifluoroacetic Acid

Vancomycin impurity.

Vancomycin impurity.
Atmosphere
Inert gas
Melting Point
>250°C (dec.)
Solubility
DMSO, Methanol, Water
Method for Determining Identity
Proton NMR (DMSO-d6) and MS
TLC Conditions
C18; Acetonitrile : Water : Acetic Acid (8: 2: 0.1). Visualized with UV and KMnO4 (Rf= 0.5).
Elemental Analysis
Calculated: 52.51% C; 4.25% H; 8.91% N Found: 48.76% C; 4.65 %H; 8.18% N
Storage and Stability
Store at -20°C under inert atmosphere. Caution: Hygroscopic. For maximum recovery of product, centrifuge the original vial prior to removing the cap.
Source
Synthetic
Purity
~98% (by HPLC)
Form
White solid
References
Mann, M., et al.: Curr. Opin. Biotechnol., 7, 11 (1996), Krone, J., et al.: Anal. Biochem., 244, 124 (1997),
USBio References
No references available
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